| ExperimentID |
EXA000001 |
| ChemicalID |
CH0001391
|
| Chemical Name |
Aspirin |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
[1] 6890N, Agilent; [2] 6890, Agilent; or others |
| Column |
[i] InertCap 5MS/NP 30 m x 0.25 mm, 0.25 μm; [ii] HP-5ms 30 m x 0.25 mm, 0.25 μm; or others |
| Column mfr. |
[I] GL Sciences; [ii] Agilent |
| Detector |
MS |
| Detector mfr. |
[1] JMS-Q1000GC K9, JEOL; [2] 5975B, Agilent |
| Ionization |
SIM-EI |
| Extraction |
SPE |
| Extraction Details |
Oasis HLB 200 mg Glass Cartridge; Eluted with Acetone |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
o-acetoxybenzoic acid-d4 |
| Syringe Spike |
Acenaphthene-d10 |
| Derivatization |
N,O-Bis(Trimethylsilyl)Trifluoroacetamide / Chlorotrimethylsilane (99:1) 200μmL; Leave it for 60 minutes at 60℃ |
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
19 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/5/17 |
