Analytical methods

ExperimentID EXA000004
ChemicalID CH0001444
Chemical Name O-Anisidine
Official Method No
Chromatography GC
Chromatography mfr. [1] 6890, Agilent; [2] 7890A Agilent; or others
Column DB-17ms 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector MS
Detector mfr. [1] 5973N, Agilent; [2] 5975C, Agilent; or others
Ionization SIM-EI
Extraction Solvent Extraction
Extraction Details Air Collection: p-aminophenol added; Sep-Pak Plus PS-2 300 L/min x 24 h; Eluted with Methanol and Dichloromethane; Extracted with diethyl ether/hexane (50:50)
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike Acenaphthene-d10
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 1.6 ng/m3
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16