| ExperimentID |
EXA000004 |
| ChemicalID |
CH0001444
|
| Chemical Name |
O-Anisidine |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
[1] 6890, Agilent; [2] 7890A Agilent; or others |
| Column |
DB-17ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
[1] 5973N, Agilent; [2] 5975C, Agilent; or others |
| Ionization |
SIM-EI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Air Collection: p-aminophenol added; Sep-Pak Plus PS-2 300 L/min x 24 h; Eluted with Methanol and Dichloromethane; Extracted with diethyl ether/hexane (50:50) |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
Acenaphthene-d10 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
1.6 ng/m3 |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
