ExperimentID |
EXA000007 |
ChemicalID |
CH0001445
|
Chemical Name |
2-Ethylhexanoic acid |
Official Method |
No |
Chromatography |
LC |
Chromatography mfr. |
[1] Nexera X2, Shimadzu; [2] Nexera XR, Shimadzu; or others |
Column |
[i] XBridge C18 150 m x 2.1 mm, 5 μm; [ii] L-column2 ODS 150 m x 2 mm, 2 μm; or others |
Column mfr. |
[i] Waters; [ii] CERI |
Detector |
MS/MS |
Detector mfr. |
[1] LCMS-8050a, Shimadzu; [2] QTRAP5500, AB Sciex ; or others |
Ionization |
SRM-ESI-negative |
Extraction |
SPE |
Extraction Details |
Oasis HLB Plus 225 mg; Eluted with Methanol |
Clean-up 1st |
|
Clean-up 1st Details |
|
Clean-up 2nd |
|
Clean-up 2nd Details |
|
Clean-up Spike |
|
Syringe Spike |
|
Derivatization |
|
Recovery Correction |
|
Instrument Detection Limit |
|
Instrument Quantification Limit |
|
Method Detection Limit |
160 ng/L |
Method Quantification Limit |
|
Repeatability |
|
Standard |
|
Recovery (CRM) |
|
Recovery (spiked) |
|
Recovery (IS) |
|
Protocol |
|
Remarks |
|
RegisterDate |
2021/3/16 |
UpdateDate |
2021/3/16 |