| ExperimentID |
EXA000008 |
| ChemicalID |
CH0001446
|
| Chemical Name |
Azilsartan |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
[1] Nexera X2, Shimadzu; [2] Nexera XR Bio, Shimadzu |
| Column |
[i] Poroshell 120 EC-C18 150 m x 2.1 mm, 4 μm; [ii] L-column2 ODS 150 m x 2.1 mm, 3 μm |
| Column mfr. |
[i] Agilent; [ii] CERI |
| Detector |
MS/MS |
| Detector mfr. |
[1] QTRAP5500, AB Sciex; [2] QTRAP4500, AB Sciex |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
Oasis MAX Plus 225 mg; Eluted with Formic acid/Methanol (2:98) |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Azilsartan-D5<_sub> |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.037 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
