Analytical methods

ExperimentID EXA000009
ChemicalID CH0001447
Chemical Name Clomipramine
Official Method No
Chromatography LC
Chromatography mfr. Nexera XR Bio, Shimadzu
Column L-column2 ODS 100 m x 2.1 mm, 3 μm
Column mfr. CERI
Detector MS/MS
Detector mfr. QTRAP4500, AB Sciex
Ionization SRM-ESI-positive
Extraction SPE
Extraction Details InertSep MC-1 500 mg; Eluted with 25% Ammonium hydroxide/Methanol (5:95)
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Clomipramine-d3
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.020 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16