| ExperimentID |
EXA000016 |
| ChemicalID |
CH0001451
|
| Chemical Name |
Trifluoroacetic acid |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
Nexera XR, Shimadzu |
| Column |
L-column2 ODS 150 mm x 2.1 mm, 5 μm |
| Column mfr. |
CERI |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP4500, AB Sciex |
| Ionization |
SRM-ESI-negative |
| Extraction |
SPE |
| Extraction Details |
Air Collection: Oasis WAXHLB Plus 225 mg x 3 pcs 0.10 L/min x 24 h; Eluted with Methanol and 0.0125% Ammonia/Methanol solution |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
Trifluoroacetic acid-13C2 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
24 ng/m3 |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
