| ExperimentID |
EXA000017 |
| ChemicalID |
CH0001452
|
| Chemical Name |
4-Tert-Butylbenzoic acid |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
1200CL, Agilent; or others |
| Column |
[i] InertSustain C18 HP 150 mm x 2.0 mm, 3 μm; [ii] Eclipse XDB-C18 150 mm x 2.1 mm, 5 μm |
| Column mfr. |
[i] GL Sciences; [ii] Agilent |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP5500, AB Sciex; or others |
| Ionization |
SRM-ESI-negative |
| Extraction |
SPE |
| Extraction Details |
Air Collection: Supelclean ENVI-8 glass hardware PTFE frit, 500 mg/6mL 0.50 L/min. x 24 h; Eluted with Acetone |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
4-Tert-Butylbenzoic acid-d13 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.21 ng/m3 |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
