Analytical methods

ExperimentID EXA000021
ChemicalID CH0001456
Chemical Name Albendazole sulfone
Official Method No
Chromatography LC
Chromatography mfr. [1] 1200, Agilent; [2] Nexera Bio, Shimadzu; or others
Column COSMOSIL PBr 150 m x 2.0 mm, 5 μm
Column mfr. Nacalai Tesque
Detector MS/MS
Detector mfr. [1] 6460, Agilent; [2] QTRAP5500, AB Sciex; or others
Ionization SRM-ESI-positive
Extraction SPE
Extraction Details Sep-Pal Plus PS-2 265 mg; Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Albendazole-d3
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 11 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16