Analytical methods

ExperimentID EXA000022
ChemicalID CH0000230
Chemical Name Benzo(a)pyrene
Official Method No
Chromatography GC
Chromatography mfr. [1] 7890A, Agilent; [2] 6890, Agilent; or others
Column [i] DB-17ms 30 m x 0.25 mm, 0.25 μm; [ii] Select PAH 30 m x 0.25 mm, 0.25 μm
Column mfr. [i] [ii] Agilent
Detector MS; HRMS
Detector mfr. [1] 5975C, Agilent; [2] AutoSpec Ultima, Waters; or others
Ionization SIM-EI
Extraction LLE
Extraction Details Extracted with Hexane
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Benzo[a] pyrene-d12
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.086 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16