ExperimentID |
EXA000022 |
ChemicalID |
CH0000230
|
Chemical Name |
Benzo(a)pyrene |
Official Method |
No |
Chromatography |
GC |
Chromatography mfr. |
[1] 7890A, Agilent; [2] 6890, Agilent; or others |
Column |
[i] DB-17ms 30 m x 0.25 mm, 0.25 μm; [ii] Select PAH 30 m x 0.25 mm, 0.25 μm |
Column mfr. |
[i] [ii] Agilent |
Detector |
MS; HRMS |
Detector mfr. |
[1] 5975C, Agilent; [2] AutoSpec Ultima, Waters; or others |
Ionization |
SIM-EI |
Extraction |
LLE |
Extraction Details |
Extracted with Hexane |
Clean-up 1st |
|
Clean-up 1st Details |
|
Clean-up 2nd |
|
Clean-up 2nd Details |
|
Clean-up Spike |
Benzo[a] pyrene-d12 |
Syringe Spike |
|
Derivatization |
|
Recovery Correction |
|
Instrument Detection Limit |
|
Instrument Quantification Limit |
|
Method Detection Limit |
0.086 ng/L |
Method Quantification Limit |
|
Repeatability |
|
Standard |
|
Recovery (CRM) |
|
Recovery (spiked) |
|
Recovery (IS) |
|
Protocol |
|
Remarks |
|
RegisterDate |
2021/3/16 |
UpdateDate |
2021/3/16 |