| ExperimentID |
EXA000023 |
| ChemicalID |
CH0000230
|
| Chemical Name |
Benzo(a)pyrene |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
[1] 6890H, Agilent; [2] 6890, Agilent |
| Column |
[i] DB-EUPAH 20 m x 0.18 mm, 0.14 μm; [ii] Select PAH 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
[i] [ii] Agilent |
| Detector |
HRMS |
| Detector mfr. |
[1] JMS-800D, JEOL; [2] AutoSpec Ultima, Waters |
| Ionization |
SIM-EI |
| Extraction |
ASE |
| Extraction Details |
Extracted with Acetone/Hexane (50:50) |
| Clean-up 1st |
LLE |
| Clean-up 1st Details |
Clean up with Hexane |
| Clean-up 2nd |
Column cleanup |
| Clean-up 2nd Details |
Sep-Pal Silica 6 cc Vac; Eluted with Dichloromethane/Hexane (5:95) |
| Clean-up Spike |
Benzo[a] pyrene-13C4 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.19 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
