Analytical methods

ExperimentID EXA000024
ChemicalID CH0001457
Chemical Name Fluvoxamine
Official Method No
Chromatography LC
Chromatography mfr. Nexera XR, Shimadzu; or others
Column [i] InertSustain C18 HP 150 m x 2.1 mm, 3 μm; [ii] L-column2 ODS 150 m x 2.1 mm, 3 μm
Column mfr. [i] GL Sciences; [ii] CERI
Detector MS/MS
Detector mfr. QTRAP5500, AB Sciex; or others
Ionization SRM-ESI-positive
Extraction SPE
Extraction Details InertSep SlimJ RP-1 for AQUA; Eluted with 28% Ammonia solution/Acetonitrile (10:90)
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 34 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16