ExperimentID |
EXA000024 |
ChemicalID |
CH0001457
|
Chemical Name |
Fluvoxamine |
Official Method |
No |
Chromatography |
LC |
Chromatography mfr. |
Nexera XR, Shimadzu; or others |
Column |
[i] InertSustain C18 HP 150 m x 2.1 mm, 3 μm; [ii] L-column2 ODS 150 m x 2.1 mm, 3 μm |
Column mfr. |
[i] GL Sciences; [ii] CERI |
Detector |
MS/MS |
Detector mfr. |
QTRAP5500, AB Sciex; or others |
Ionization |
SRM-ESI-positive |
Extraction |
SPE |
Extraction Details |
InertSep SlimJ RP-1 for AQUA; Eluted with 28% Ammonia solution/Acetonitrile (10:90) |
Clean-up 1st |
|
Clean-up 1st Details |
|
Clean-up 2nd |
|
Clean-up 2nd Details |
|
Clean-up Spike |
|
Syringe Spike |
|
Derivatization |
|
Recovery Correction |
|
Instrument Detection Limit |
|
Instrument Quantification Limit |
|
Method Detection Limit |
34 ng/L |
Method Quantification Limit |
|
Repeatability |
|
Standard |
|
Recovery (CRM) |
|
Recovery (spiked) |
|
Recovery (IS) |
|
Protocol |
|
Remarks |
|
RegisterDate |
2021/3/16 |
UpdateDate |
2021/3/16 |