| ExperimentID |
EXA000029 |
| ChemicalID |
CH0001611
|
| Chemical Name |
Linear tetradecylbenzene sulphonate |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
ACQUITY UPLC, Waters |
| Column |
L-column2 ODS 150 m x 2.1 mm, 3 μm |
| Column mfr. |
CERI |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP550, AB Sciex |
| Ionization |
SRM-ESI-negative |
| Extraction |
Solvent extraction |
| Extraction Details |
Eluted with Methanol |
| Clean-up 1st |
SPE |
| Clean-up 1st Details |
InertSep GC 500 mg/ 6 mL; Eluted with Ammonia-containing acetone/Hexane/Toluene (28% Ammonia water + Acetone + Hexane + Toluene (30:65:5)) |
| Clean-up 2nd |
SPE |
| Clean-up 2nd Details |
InertSep C18-ENV 500 mg / 6 mL; Eluted with Dipropylammonium Acetate/Methanol solution |
| Clean-up Spike |
4-Sodium dodecylbenzene sulfonate |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
2.0 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
