| ExperimentID |
EXA000031 |
| ChemicalID |
CH0001439
|
| Chemical Name |
Permethrin |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
7890B, Agilent; or others |
| Column |
DB-17ms 30 m x 0.25 mm, 0.25 μm; or others |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
JMS-Q1500GC, JEOL; or others |
| Ionization |
SIM-EI |
| Extraction |
Solvent extraction |
| Extraction Details |
Extracted with Hexane 50 mL x 10 min. and then Hexane 20 mL x 10 min. |
| Clean-up 1st |
Column cleanup |
| Clean-up 1st Details |
Sep-Pak Silica 690 mg; Eluted with Diethyl ether/Hexane (2:98); This clean up process was added if the sample included lots of interfering substances. |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Permethrin-d5 |
| Syringe Spike |
Perylene-d12; Polyethylene glycol |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.31 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
