| ExperimentID |
EXA000033 |
| ChemicalID |
CH0001439
|
| Chemical Name |
Permethrin |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
7890B, Agilent; or others |
| Column |
DB-17ms 30 m x 0.25 mm, 0.25 μm; or others |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
JMS-Q1500GC, JEOL; or others |
| Ionization |
SIM-EI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Extracted with Acetone and then with Hexane |
| Clean-up 1st |
Column cleanup |
| Clean-up 1st Details |
ENVI-Carb 250 mg; Eluted with Hexane |
| Clean-up 2nd |
Column cleanup |
| Clean-up 2nd Details |
Sep-Pak Silica 690 mg; Eluted with Diethyl ether/Hexane (2:98) |
| Clean-up Spike |
Permethrin-d5 |
| Syringe Spike |
Perylene-d12; Polyethylene glycol |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.22 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
