| ExperimentID |
EXA000035 |
| ChemicalID |
CH0001579
|
| Chemical Name |
N,N-Dimethylformamide |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
6890, Agilent; or others |
| Column |
[i] BP-20 30 m x 0.25 mm, 0.25 μm; [ii] InertCap Pure WAX 30 m x 0.25 mm, 0.25 μm; or others |
| Column mfr. |
[i] SGE; [ii] GL Sciences |
| Detector |
MS |
| Detector mfr. |
JMS-Q100GC K9, JEOL; or others |
| Ionization |
SIM-MEI |
| Extraction |
SPE |
| Extraction Details |
Serially-coupled columns: Sep-Pak C18 and Sep-Pak AC2; Eluted with Acetone and Dichloromethane (only from Sep-Pak AC2) |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
N,N-Dimethylformamide-13C2 |
| Syringe Spike |
N,N-Dimethylformamide-d7 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
59 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
