| ExperimentID |
EXA000036 |
| ChemicalID |
CH0001580
|
| Chemical Name |
Thiocyanic acid and its solts |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
GC-2010 Plus, Shimadzu |
| Column |
Rtx-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
RESTEK |
| Detector |
MS |
| Detector mfr. |
GCMS-TQ8030, Shimadzu |
| Ionization |
SIM-MEI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Extracted with Ethyl acetate |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
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| Syringe Spike |
|
| Derivatization |
Phosphate buffer 1 mL and 0.1 mol/L Benzyldimethyltetradecylammonium chloride aqueous solution 700 μL; Pentafluorobenzyl Bromide/Toluene (10:90) 2 mL |
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
1.1 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
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| Recovery (IS) |
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| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
