Analytical methods

ExperimentID EXA000058
ChemicalID CH0001602
Chemical Name Heptachloroheptadecane
Official Method No
Chromatography LC
Chromatography mfr. 1200SL, Agilent
Column Inertsil C4 250 mm x 4.0 mm, 5 μm
Column mfr. GL Sciences
Detector MS/MS
Detector mfr. 6460, Agilent
Ionization SRM-ESI-negative
Extraction Solvent Extraction
Extraction Details Extracted with Sodium chloride, Dichloromethane
Clean-up 1st Column cleanup
Clean-up 1st Details 44% Silica gel sulfate; Florisil (Magnesium silicate); Eluted with Dichloromethane/Hexane (20:80)
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.61 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16