| ExperimentID |
EXA000082 |
| ChemicalID |
CH0001602
|
| Chemical Name |
Heptachloroheptadecane |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
1200SL, Agilent |
| Column |
Inertsil C4 250 mm x 4.0 mm, 5 μm |
| Column mfr. |
GL Sciences |
| Detector |
MS/MS |
| Detector mfr. |
6460, Agilent |
| Ionization |
SRM-ESI-negative |
| Extraction |
Soxhlet Extraction |
| Extraction Details |
Extracted with Toluene |
| Clean-up 1st |
Solvent Extraction |
| Clean-up 1st Details |
Extracted with Hexane saturated acetonitrile, and then with Hexane |
| Clean-up 2nd |
Column cleanup |
| Clean-up 2nd Details |
44% Silica gel sulfate; Florisil (Magnesium silicate); Eluted with Dichloromethane/Hexane (20:80) |
| Clean-up Spike |
|
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.97 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
