| ExperimentID |
EXA000085 |
| ChemicalID |
CH0000812
|
| Chemical Name |
Hydrazine |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
[1] GCMS-QP2010 Plus, Shimadzu; [2] 6890N, Agilent; [3] GC-2010 Plus, Shimadzu |
| Column |
[i] DB-5ms 30 m x 0.25 mm, 0.25 μm; [ii] Supelco SLB-5ms 30 m x 0.25 mm, 0.25 μm; [iii] Rtx-5ms 30 m x 0.25 mm, 2.5 μm |
| Column mfr. |
[i] Agilent; [ii] Sigma-Aldrich; [iii] RESTEK |
| Detector |
MS |
| Detector mfr. |
[2] JMS-Q1000GC K9, JEOL; [3] GCMS-TQ8030, Shimadzu; |
| Ionization |
SIM-EI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Extracted with Hexane |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Hydrazine sulfate-15N2 |
| Syringe Spike |
Acenaphtene-d10 |
| Derivatization |
1% Pentafluorobenzaldehyde aqueous solution 30 mL; Shake it for 10 min. and leave it for 16 h. |
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.0096 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
