| ExperimentID |
EXA000086 |
| ChemicalID |
CH0000812
|
| Chemical Name |
Hydrazine |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
6890N, Agilent |
| Column |
DB-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
[1]MS; [2]MS/MS |
| Detector mfr. |
JMS-Q1000GC K9, JEOL |
| Ionization |
[1] SIM-EI; [2] SRM-EI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Air Collection: Polycarbonate absorption bulb (0.1% Phosphoric acid aqueous solution + 0.1% Sodium thiosulfate aqueous solution); Extracted with Hexane |
| Clean-up 1st |
Salting out |
| Clean-up 1st Details |
Sodium chloride and purified water |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Hydrazine sulfate-15N2 |
| Syringe Spike |
Acenaphtene-d10 |
| Derivatization |
1% Pentafluorobenzaldehyde aqueous solution 30 mL; Shake it for 10 min. and leave it for 16 h. |
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.33 ng/m3 |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
