| ExperimentID |
EXA000087 |
| ChemicalID |
CH0001605
|
| Chemical Name |
(1-Hydroxyethane-1,1-diyl)diphosphonic acid and its solts |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
ACQUITY UPLC H-Class, Waters |
| Column |
HILICpak VG-50 2D 150 m x 2.0 mm, 5 μm |
| Column mfr. |
Shodex |
| Detector |
MS/MS |
| Detector mfr. |
Xevo TQD, Waters |
| Ionization |
SRM-ESI-Positive |
| Extraction |
|
| Extraction Details |
|
| Clean-up 1st |
Column cleanup |
| Clean-up 1st Details |
Serially-coupled columns: TOYOPAK IC-SP 1.0 mL and DISMIC-13HP; The first 1.5mL of spilled water: discarded; The rest of it: used as the test solution |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
3300 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2021/3/16 |
| UpdateDate |
2021/3/16 |
