Analytical methods

ExperimentID EXA000089
ChemicalID CH0001606
Chemical Name n-Hexane
Official Method No
Chromatography Head space GC
Chromatography mfr. GCMS-QP2010 Ultra, Shimadzu equipped with HS-20, Shimadzu; or others
Column Rtx-5ms 30 m x 0.32 mm, 1.8 μm; or others
Column mfr. RESTEK
Detector MS
Detector mfr. GCMS-QP2010 Ultra, Shimadzu; or others
Ionization SIM-EI
Extraction
Extraction Details
Clean-up 1st Salting out
Clean-up 1st Details Sodium chloride
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Hexane-d14
Syringe Spike Fluorobenzene
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 1.1 ng/g dry
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol
Remarks
RegisterDate 2021/3/16
UpdateDate 2021/3/16