Analytical methods

ExperimentID EXA000134
ChemicalID CH0000372
Chemical Name PFOA
Official Method No
Chromatography LC
Chromatography mfr. ACQUITY UPLC I-Class, Waters
Column BEH C18 50 m x 2.1 mm, 1.7 μm
Column mfr. Waters
Detector MS/MS
Detector mfr. API-6500, AB Sciex
Ionization SRM-ESI-negative
Extraction SPE
Extraction Details Presep-C Agri; Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 13C4PFOA
Syringe Spike NA
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 30 pg/L
Method Quantification Limit 70 pg/L
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2019/shosai/3_7.pdf
Remarks Analysis method: p.446
RegisterDate 2021/5/21
UpdateDate 2021/5/21