| ExperimentID |
EXA000277 |
| ChemicalID |
CH0001174
|
| Chemical Name |
Hexachloro-1,3-butadiene |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
HP 6890, Agilent |
| Column |
DB-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
HP 5973, Agilent |
| Ionization |
SIM-EI |
| Extraction |
Thermal Desorption (TD) |
| Extraction Details |
Collection Tube for TD: Tenax TA |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
13C6-Pentachlorobenzene |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
10 pg/m3 |
| Method Quantification Limit |
30 pg/m3 |
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2019/shosai/3_7.pdf |
| Remarks |
Analysis method: p.450 |
| RegisterDate |
2021/6/04 |
| UpdateDate |
2021/6/04 |
