Analytical methods

ExperimentID EXA000279
ChemicalID CH0001175
Chemical Name Pentachloroanisole
Official Method No
Chromatography GC
Chromatography mfr. 7890A, Agilent
Column HP-5msI 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector HRMS
Detector mfr. AutoSpec Premier, Waters
Ionization SIM-EI
Extraction Soxhlet Extraction
Extraction Details Air collection: QFF, PUF and ACF; Extracted with Acetone and Toluene (QFF, ACF), with Acetone (PUF)
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 13C6Pentachloroanisole
Syringe Spike 13C12-PCB#52
Derivatization N,O-Bis(Trimethylsilyl)Trifluoroacetamide
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.4 pg/m3
Method Quantification Limit 1.1 pg/m3
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.453; Resolution: 10,000
RegisterDate 2021/6/04
UpdateDate 2021/6/04