| ExperimentID |
EXA000289 |
| ChemicalID |
CH0001614
|
| Chemical Name |
Cybutryne |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
LC-30AD Prominence system, Shimadzu |
| Column |
ODS-4 column 2.1 mm i.d. x 150 mm, 5 μm; equipped with a Unixon UK-C18 guard cartridge 3 mm i.d. x 5 mm, 3 μm |
| Column mfr. |
GL Science Inc; Imtakt |
| Detector |
MS |
| Detector mfr. |
LCMS-8030, Shimadzu |
| Ionization |
Electrospray ionization in the positive-ion mode |
| Extraction |
SPE |
| Extraction Details |
Filtered with GF/C filter, Whatman; Extracted with Oasis HLB plus LP (186000132, Nihon Waters K.K); Eluted with methanol; Transported to the laboratory and stored at 4℃ until chemical analysis; SPE was conducted in the laboratory within 48 h.; 6 N hydrochlorie (1ml per L of samle) was added on site to preveny degradation; |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
atrazine-13C3 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
|
| Method Quantification Limit |
0.1 ng/L |
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
117% |
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
2019 samples |
| RegisterDate |
2021/12/14 |
| UpdateDate |
2021/12/14 |
