| ExperimentID |
EXA000303 |
| ChemicalID |
CH0000660
|
| Chemical Name |
Thallium |
| Official Method |
No |
| Chromatography |
|
| Chromatography mfr. |
|
| Column |
|
| Column mfr. |
|
| Detector |
ICP-MS |
| Detector mfr. |
7800, Agilent |
| Ionization |
|
| Extraction |
|
| Extraction Details |
|
| Clean-up 1st |
Heat treatment |
| Clean-up 1st Details |
Concentrated nitric acid 5mL, Heated at 95 ℃ and concentrate 100mL sample to 50-70mL |
| Clean-up 2nd |
Filtration |
| Clean-up 2nd Details |
Filtered with Fiter paper No. 5B, Advantec |
| Clean-up Spike |
|
| Syringe Spike |
Bismuth |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.14 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_1_2.pdf |
| Remarks |
Fresh water samples; Analysis method: p.6 |
| RegisterDate |
2022/1/25 |
| UpdateDate |
2022/1/25 |
