| ExperimentID |
EXA000306 |
| ChemicalID |
CH0000315
|
| Chemical Name |
Tiamulin |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
LC-20A, Shimadzu; LC-30A Series, Shimadzu |
| Column |
Poroshell 120 EC-C18 50mm x 2.1mm, 2.7μm |
| Column mfr. |
Agilent |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP4500, AB Sciex; 8050, Shimadzu |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
Sep-Pak Plus PS-2 265mg 10mL/min.; Eluted with Acetonitrile |
| Clean-up 1st |
Washing |
| Clean-up 1st Details |
Cartridge: Washed with purified water |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Tiamulin-d10 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.013 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.7 |
| RegisterDate |
2022/1/25 |
| UpdateDate |
2022/1/25 |
