| ExperimentID |
EXA000310 |
| ChemicalID |
CH0001628
|
| Chemical Name |
Pyrimethanil |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
1200, Agilent; LC-30A Series, Shimadzu |
| Column |
Poroshell 120 EC-C18 150mm x 2.1mm, 2.7μm |
| Column mfr. |
Agilent |
| Detector |
MS/MS |
| Detector mfr. |
6460 Jet Stream, Agilent; 8050, Shimadzu |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
Oasis HLB Plus 225 mg/10 mL/min; Eluted with Methanol |
| Clean-up 1st |
Filtration |
| Clean-up 1st Details |
Only samples incluing a lot of suspension: Filtered with GF/C, Whatman |
| Clean-up 2nd |
Washing |
| Clean-up 2nd Details |
Cartridge: Washed with purified water |
| Clean-up Spike |
Pyrimethanil-d5 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
2.1 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.1 |
| RegisterDate |
2022/1/25 |
| UpdateDate |
2022/1/25 |
