Analytical methods
| ExperimentID | EXA000318 |
|---|---|
| ChemicalID | CH0000660 |
| Chemical Name | Thallium |
| Official Method | No |
| Chromatography | |
| Chromatography mfr. | |
| Column | |
| Column mfr. | |
| Detector | ICP-MS |
| Detector mfr. | 7700, Agilent |
| Ionization | |
| Extraction | Solvent Extraction |
| Extraction Details | Air Collection:Quartz fiber filter paper 700L/min. x 24h; Preparatory: Divide the filter paper into 8 equal parts; use two of them; Heat acid decomposition; Diluted with 2% nitric acid |
| Clean-up 1st | |
| Clean-up 1st Details | |
| Clean-up 2nd | |
| Clean-up 2nd Details | |
| Clean-up Spike | |
| Syringe Spike | Rhenium |
| Derivatization | |
| Recovery Correction | |
| Instrument Detection Limit | |
| Instrument Quantification Limit | |
| Method Detection Limit | 0.00020 ng/m3 |
| Method Quantification Limit | |
| Repeatability | |
| Standard | |
| Recovery (CRM) | |
| Recovery (spiked) | |
| Recovery (IS) | |
| Protocol | https://www.env.go.jp/chemi/kurohon/2020/shosai/5_1_2.pdf |
| Remarks | Analysis method: p.6 |
| RegisterDate | 2022/2/22 |
| UpdateDate | 2022/2/22 |