Analytical methods

ExperimentID EXA000320
ChemicalID CH0001626
Chemical Name N-nitrosodimethylamine
Official Method No
Chromatography GC
Chromatography mfr. 7890B, Agilent
Column Pure WAX 30m x 0.25mm, 0.25μm
Column mfr. InertCap
Detector HRMS
Detector mfr. JMS 800D, JEOL
Ionization SIM-EI
Extraction SPE
Extraction Details Sep-Pak Plus AC-2 400mg/80μm 0.70L/min. x 24h; Eluted with Acetone and Dichloromethane
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike N-nitrosodimethylamine-13C2,d8
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.0075 ng/m3
Method Quantification Limit
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.8
RegisterDate 2022/2/22
UpdateDate 2022/2/22