Analytical methods

ExperimentID EXA000321
ChemicalID CH0001055
Chemical Name Pyridine
Official Method No
Chromatography GC
Chromatography mfr. 6890 GC, Agilent
Column TG-WAXMS B 60m x 0.25mm, 0.25μm; (Two 30m-columns connected with a column connector)
Column mfr. TraceGOLD
Detector MS
Detector mfr. JMS-K9, JEOL
Ionization SIM-EI
Extraction SPE
Extraction Details InertSep RP-1 mini (Three columns connected in series), 0.3L/min. x 24h; Eluted with Acetone
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike Pyridine-d5
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 2.4 ng/m3
Method Quantification Limit
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.9
RegisterDate 2022/2/22
UpdateDate 2022/2/22