| ExperimentID |
EXA000322 |
| ChemicalID |
CH0001632
|
| Chemical Name |
Isocyanuric acid |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
1260, Agilent |
| Column |
Asahipak NH2P-40 2D 150 mm x 2.0 mm, 4 μm |
| Column mfr. |
Shodex |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP 6500, AB Sciex |
| Ionization |
SRM-ESI-negative |
| Extraction |
SPE |
| Extraction Details |
ISOLUTE ENV+ 500 mg/6 mL 10 mL/min; Eluted with Acetonitrile and purified water (50:50) 5 mL |
| Clean-up 1st |
Filtration |
| Clean-up 1st Details |
Filtered with 0.45 μm membrane filter |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Isocyanuric acid- 13C3 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
500 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.1 |
| RegisterDate |
2022/5/06 |
| UpdateDate |
2022/5/06 |
