| ExperimentID |
EXA000324 |
| ChemicalID |
CH0001633
|
| Chemical Name |
14-(R)-Hydroxyclarithromycin |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
[1]ACQUITY UPLC, Waters; [2]1260, Agilent |
| Column |
Atiantis T3 150 mm x 2.1 mm, 3 μm |
| Column mfr. |
Waters |
| Detector |
MS/MS |
| Detector mfr. |
[1]Xevo TQ, Waters; [2]QTRAP 4500; AB Sciex |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
Oass HLB Plus 225 mg Short 10 mL/min; Eluted with Methanol |
| Clean-up 1st |
Filtration |
| Clean-up 1st Details |
Filtered with LH filter 0.45 μm; Hydrophilic PTFE 13 mm, Millex |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.62 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.3 |
| RegisterDate |
2022/5/06 |
| UpdateDate |
2022/5/06 |
