| ExperimentID |
EXA000325 |
| ChemicalID |
CH0000809
|
| Chemical Name |
2,6-Di-tert-butyl-4-methylphenol |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
6890, Agilent |
| Column |
[i]J&W Ultra2 25 m x 0.2 mm, 0.33 μm; [ii]J&W DB-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
[i][ii]Agilent |
| Detector |
MS |
| Detector mfr. |
JEOL JMS-800 |
| Ionization |
SIM-EI |
| Extraction |
SPE |
| Extraction Details |
Supelclean ENVI-18 20 mL/min; Eluted with Hexane |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Hexachlorobenzene- 13C6 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
35 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.3 |
| RegisterDate |
2022/5/06 |
| UpdateDate |
2022/5/06 |
