| ExperimentID |
EXA000326 |
| ChemicalID |
CH0001634
|
| Chemical Name |
N-[3-(Dimethylamino)propyl]stearamide |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
Exion LC, Sciex |
| Column |
C18 150 mm x 2.1 mm, 3 μm |
| Column mfr. |
InertSustain |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP 6500, Sciex |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
InertSep C18 300 mg/3 mL 5 mL/min; Eluted with Methanol |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
1.6 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.5 |
| RegisterDate |
2022/5/06 |
| UpdateDate |
2022/5/06 |
