Analytical methods

ExperimentID EXA000328
ChemicalID CH0000810
Chemical Name N,N-Dimethyldodecyl-1-amine N-oxide
Official Method No
Chromatography LC
Chromatography mfr. 1260, Agilent
Column C18 150 mm x 2.1 mm, 3 μm
Column mfr. InertSustain
Detector MS/MS
Detector mfr. QTRAP 4500, AB Sciex
Ionization SRM-ESI-positive
Extraction SPE
Extraction Details SDB-XD 47 mm 20 mL/min; Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 7.6 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf
Remarks Analysis method: p.6
RegisterDate 2022/5/06
UpdateDate 2022/5/06