ExperimentID |
EXA000328 |
ChemicalID |
CH0000810
|
Chemical Name |
N,N-Dimethyldodecyl-1-amine N-oxide |
Official Method |
No |
Chromatography |
LC |
Chromatography mfr. |
1260, Agilent |
Column |
C18 150 mm x 2.1 mm, 3 μm |
Column mfr. |
InertSustain |
Detector |
MS/MS |
Detector mfr. |
QTRAP 4500, AB Sciex |
Ionization |
SRM-ESI-positive |
Extraction |
SPE |
Extraction Details |
SDB-XD 47 mm 20 mL/min; Eluted with Methanol |
Clean-up 1st |
|
Clean-up 1st Details |
|
Clean-up 2nd |
|
Clean-up 2nd Details |
|
Clean-up Spike |
|
Syringe Spike |
|
Derivatization |
|
Recovery Correction |
|
Instrument Detection Limit |
|
Instrument Quantification Limit |
|
Method Detection Limit |
7.6 ng/L |
Method Quantification Limit |
|
Repeatability |
|
Standard |
|
Recovery (CRM) |
|
Recovery (spiked) |
|
Recovery (IS) |
|
Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
Remarks |
Analysis method: p.6 |
RegisterDate |
2022/5/06 |
UpdateDate |
2022/5/06 |