| ExperimentID |
EXA000331 |
| ChemicalID |
CH0001638
|
| Chemical Name |
N,N'-Ethylenebis(dithiocarbamamic acid) |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
1260, Agilent |
| Column |
RP-Amide 100 mm x 2.1 mm, 3 μm |
| Column mfr. |
Ascentis |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP 4500, AB Sciex |
| Ionization |
SRM-ESI-negative |
| Extraction |
SPE |
| Extraction Details |
Oass HLB; Eluted with Acetonitrile |
| Clean-up 1st |
Filtration |
| Clean-up 1st Details |
Filtered with Glass fiber filter paper: Whatman GF/B 60 mm |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
|
| Derivatization |
Dimethyl sulfate 400 μL 0.6 mol/L Hydrochloric acid aqueous solution 12 mL; Shaken for 10 min.; left for 20 min. |
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.76 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.6 |
| RegisterDate |
2022/5/06 |
| UpdateDate |
2022/5/06 |
