| ExperimentID |
EXA000333 |
| ChemicalID |
CH0000809
|
| Chemical Name |
2,6-Di-tert-butyl-4-methylphenol |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
6890, Agilent |
| Column |
J&W DB-5ms 30m x 0.25mm, 0.25μm |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
5975, Agilent |
| Ionization |
SIM-EI |
| Extraction |
Solvent |
| Extraction Details |
Extracted with Acetone (15min), Sonicated for 15min., then Centrifugated (2,000rpm, 5min.), Repeated these twice |
| Clean-up 1st |
Column cleanup |
| Clean-up 1st Details |
LC-Florisil; Eluted with Hexane |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
2,6-Di-tert-butyl-4-methylphenol-d24 |
| Syringe Spike |
Hexachlorobenzene- 13C6 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.070 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.4 |
| RegisterDate |
2022/5/13 |
| UpdateDate |
2022/5/13 |
