Analytical methods

ExperimentID EXA000333
ChemicalID CH0000809
Chemical Name 2,6-Di-tert-butyl-4-methylphenol
Official Method No
Chromatography GC
Chromatography mfr. 6890, Agilent
Column J&W DB-5ms 30m x 0.25mm, 0.25μm
Column mfr. Agilent
Detector MS
Detector mfr. 5975, Agilent
Ionization SIM-EI
Extraction Solvent
Extraction Details Extracted with Acetone (15min), Sonicated for 15min., then Centrifugated (2,000rpm, 5min.), Repeated these twice
Clean-up 1st Column cleanup
Clean-up 1st Details LC-Florisil; Eluted with Hexane
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 2,6-Di-tert-butyl-4-methylphenol-d24
Syringe Spike Hexachlorobenzene- 13C6
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.070 ng/g dry
Method Quantification Limit
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.4
RegisterDate 2022/5/13
UpdateDate 2022/5/13