Analytical methods

ExperimentID EXA000334
ChemicalID CH0001634
Chemical Name N-[3-(Dimethylamino)propyl]stearamide
Official Method No
Chromatography LC
Chromatography mfr. Exion LC, Sciex
Column C18 150mm x 2.1mm, 3μm
Column mfr. InertSustain
Detector MS/MS
Detector mfr. QTRAP 6500, Sciex
Ionization SRM-ESI-positive
Extraction Solvent; SPE
Extraction Details Solvent: Extracted with Methanol, Shaken for 20 min., then Centrifugated (3,000rpm, 20 min.), Repeated these three times; SPE: InertSep C18 (300mg/3mL 5mL/min); Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 6.1 ng/g dry
Method Quantification Limit
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.5
RegisterDate 2022/5/13
UpdateDate 2022/5/13