Analytical methods
| ExperimentID | EXA000334 |
|---|---|
| ChemicalID | CH0001634 |
| Chemical Name | N-[3-(Dimethylamino)propyl]stearamide |
| Official Method | No |
| Chromatography | LC |
| Chromatography mfr. | Exion LC, Sciex |
| Column | C18 150mm x 2.1mm, 3μm |
| Column mfr. | InertSustain |
| Detector | MS/MS |
| Detector mfr. | QTRAP 6500, Sciex |
| Ionization | SRM-ESI-positive |
| Extraction | Solvent; SPE |
| Extraction Details | Solvent: Extracted with Methanol, Shaken for 20 min., then Centrifugated (3,000rpm, 20 min.), Repeated these three times; SPE: InertSep C18 (300mg/3mL 5mL/min); Eluted with Methanol |
| Clean-up 1st | |
| Clean-up 1st Details | |
| Clean-up 2nd | |
| Clean-up 2nd Details | |
| Clean-up Spike | |
| Syringe Spike | |
| Derivatization | |
| Recovery Correction | |
| Instrument Detection Limit | |
| Instrument Quantification Limit | |
| Method Detection Limit | 6.1 ng/g dry |
| Method Quantification Limit | |
| Repeatability | |
| Standard | |
| Recovery (CRM) | |
| Recovery (spiked) | |
| Recovery (IS) | |
| Protocol | https://www.env.go.jp/chemi/kurohon/2020/shosai/5_2_2.pdf |
| Remarks | Analysis method: p.5 |
| RegisterDate | 2022/5/13 |
| UpdateDate | 2022/5/13 |