Analytical methods

ExperimentID EXA000389
ChemicalID CH0001175
Chemical Name Pentachloroanisole
Official Method No
Chromatography GC
Chromatography mfr. 6890, Agilent; 7683, Agilent
Column DB-5ms 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector HRMS
Detector mfr. AutoSpec Ultima, Waters; AutoSpec Premier, Waters
Ionization SIM-EI
Extraction Solvent Extraction
Extraction Details Extracted with Dichloromethane
Clean-up 1st Multilayer column cleanup
Clean-up 1st Details Silica gel, Anhydrous sodium sulfate; Eluted with Dichloromethane
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 13C12-Pentachloroanisole
Syringe Spike 13C12-PCB#9, #19, #70, #111, #155, #178, or #202 and Decane
Derivatization N,O-Bis(Trimethylsilyl)Trifluoroacetamide
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 10 pg/L
Method Quantification Limit 30 pg/L
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.15; Resolution: 10,000
RegisterDate 2022/6/02
UpdateDate 2022/6/02