| ExperimentID |
EXA000394 |
| ChemicalID |
CH0001520
|
| Chemical Name |
Dicofol |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
6890, Agilent; 7683, Agilent |
| Column |
DB-5ms 15 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
HRMS |
| Detector mfr. |
AutoSpec Ultima, Waters; AutoSpec Premier, Waters |
| Ionization |
SIM-EI |
| Extraction |
Solvent Extraction |
| Extraction Details |
Extracted with Dichloromethane |
| Clean-up 1st |
Multilayer column cleanup |
| Clean-up 1st Details |
Florisil, Anhydrous sodium sulfate; Eluted with Dichloromethane/Hexane (50:50) |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Dicofol-d8 |
| Syringe Spike |
13C12-PCB#9, #19, #70, #111, #155, #178, or #202 and Decane |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
8 pg/L |
| Method Quantification Limit |
13 pg/L |
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2020/shosai/5_3_2.pdf |
| Remarks |
Analysis method: p.15; Resolution: 10,000 |
| RegisterDate |
2022/6/02 |
| UpdateDate |
2022/6/02 |
