| ExperimentID |
EXA000518 |
| ChemicalID |
CH0000724
|
| Chemical Name |
TBEP |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
7890 series, Agilent |
| Column |
DB17-HT column 30 m x 0.25 mm x 0.15 μm |
| Column mfr. |
Agilent |
| Detector |
MS/MS |
| Detector mfr. |
7000 GC/MS Triple Quad, Agilent |
| Ionization |
|
| Extraction |
ASE |
| Extraction Details |
Extracted with a mixture of Hexane and acetone (1:1, v/v) using a SE-100 High-Speed Solvent Extractor (Mitsubishi Chemical Analytech, Japan), running at 35 ℃, at 6 mL/min for 30 min. |
| Clean-up 1st |
SPE |
| Clean-up 1st Details |
Single step: [1] SPE step using Supelclean TM ENVI-Carb TM SPE cartoridge (250 mg/6 mL, Sigma-Aldrich) conditioned with 25 mL acetone/hexane mixture (1:1, v/v), loaded with sample extract; Eluted with 20 mL acetone/hexane (1:1, v/v) |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
d33-IPP; d12-TCEP; d18-TCIPP; d15-TDCIPP; d15-TPHP; 13C6-TBOEP; 13C18-TPHP |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
670-1600 ng/g dry |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
2022/8/08 |
| UpdateDate |
2022/8/08 |
