Analytical methods

ExperimentID EXA000580
ChemicalID CH0001174
Chemical Name Hexachloro-1,3-butadiene
Official Method No
Chromatography GC
Chromatography mfr. HP 6890, Agilent
Column DB-5ms 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector MS
Detector mfr. HP 5973, Agilent
Ionization SIM-EI
Extraction Thermal Desorption (TD)
Extraction Details Collection Tube for TD: Tenax TA
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike 13C6-Pentachlorobenzene
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 20 pg/m3
Method Quantification Limit 50 pg/m3
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2020/shosai/5_3_2.pdf
Remarks Analysis method: p.14
RegisterDate 2022/9/27
UpdateDate 2022/9/27