| ExperimentID |
EXA000591 |
| ChemicalID |
CH0000274
|
| Chemical Name |
Clofibric acid |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
[1] ACQUITY UPLC H-Class, Waters; [2] Necera XR, Shimadzu |
| Column |
CORTECS UPLC C18 100 mm x 2.1 mm, 1.6 μm |
| Column mfr. |
Waters |
| Detector |
MS/MS |
| Detector mfr. |
[1] Xevo TQD, Waters; [2] LCMS-8050, Shimadzu |
| Ionization |
SRM-ESI-negative |
| Extraction |
SPE |
| Extraction Details |
Oasis HLB; Eluted with Methanol |
| Clean-up 1st |
Washing |
| Clean-up 1st Details |
Washed in purified water |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Clofibric acid-d4 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
33 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.2 |
| RegisterDate |
2022/10/17 |
| UpdateDate |
2022/10/17 |
