| ExperimentID |
EXA000592 |
| ChemicalID |
CH0001655
|
| Chemical Name |
Hexachloroethane |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
[1] 6890N, Agilent; [2] 8890, Agilent |
| Column |
HP-5ms UI 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
HRMS |
| Detector mfr. |
[1] 5975C, Agilent; [2] JMS-Q1500, JEOL |
| Ionization |
SIM-EI |
| Extraction |
Solvent extraction |
| Extraction Details |
Extracted with Sodium chloride (Fresh water only), Dichloromethane, shaken twice |
| Clean-up 1st |
Column Cleanup |
| Clean-up 1st Details |
LC-Si Glass Tubes, Eluted with Hexane |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
naphthalene-d8; p-Bromofluorobenzene |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.55 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.2 |
| RegisterDate |
2022/10/17 |
| UpdateDate |
2022/10/17 |
