| ExperimentID |
EXA000597 |
| ChemicalID |
CH0001661
|
| Chemical Name |
2-Ethylhexyl methacrylate |
| Official Method |
No |
| Chromatography |
Head space GC |
| Chromatography mfr. |
GCMS-QP2010, Shimadzu equipped with Turbomatrix-40, Perkin Elmer |
| Column |
Rtx-624 60 m x 0.32 mm, 1.8 μm |
| Column mfr. |
RESTEK |
| Detector |
MS |
| Detector mfr. |
GCMS-QP2010, Shimadzu |
| Ionization |
SIM-EI |
| Extraction |
|
| Extraction Details |
|
| Clean-up 1st |
Salting out |
| Clean-up 1st Details |
Sodium chloride |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
|
| Syringe Spike |
2,2,3,3-Tetrafluoropropyl Acrylate-1-13C,2,3,3-d3 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
12 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.4 |
| RegisterDate |
2022/10/17 |
| UpdateDate |
2022/10/17 |
