| ExperimentID |
EXA000598 |
| ChemicalID |
CH0001662
|
| Chemical Name |
Dichlorvos |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
[1] Nexera X2, Shimadzu; [2] Necera XR, Shimadzu |
| Column |
X-Bridge C18 150 mm x 2.1 mm, 3.5 μm |
| Column mfr. |
Waters |
| Detector |
MS/MS |
| Detector mfr. |
[1] LCMS-8050, Shimadzu; [2] QTRAP 4500, AB Sciex |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
Sep-Pak PS2 Plus Short Cartridge; Eluted with Acetonitrile |
| Clean-up 1st |
Washing |
| Clean-up 1st Details |
Washed in purified water/Methanol (50:50) |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Dichlorvos-d6 |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.43 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_1_2.pdf |
| Remarks |
Analysis method: p.5 |
| RegisterDate |
2022/10/17 |
| UpdateDate |
2022/10/17 |
