Analytical methods

ExperimentID EXA000599
ChemicalID CH0001660
Chemical Name Triglycidyl isocyanurate
Official Method No
Chromatography LC
Chromatography mfr. ExionLC, AB Sciex
Column CORTECS C18+ 150 mm x 2.1 mm, 2.7 μm
Column mfr. Waters
Detector MS/MS
Detector mfr. Triple Quad 4500 System, AB Sciex
Ionization SRM-ESI-positive
Extraction
Extraction Details Air collection: Sep-Pak Silica Plus Long Cartridge, 690 mg 0.5L/min. x 24h.; Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.039 ng/m3
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_1_2.pdf
Remarks Analysis method: p.4
RegisterDate 2022/10/17
UpdateDate 2022/10/17