Analytical methods

ExperimentID EXA000601
ChemicalID CH0000907
Chemical Name Aniline
Official Method No
Chromatography GC
Chromatography mfr. 8890, Agilent
Column J&W DB-WAX 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector MS
Detector mfr. 5977B, Agilent
Ionization SIM-EI
Extraction SPE
Extraction Details Sep-Pak PS-2 Plus; Eluted with Methyl acetate
Clean-up 1st Washing
Clean-up 1st Details Washed in purified water
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Aniline-d5
Syringe Spike Naphthalene-d8
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 14 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf
Remarks Analysis method: p.1
RegisterDate 2022/11/25
UpdateDate 2022/11/25